solid-phase相关论文
Solid-phase isotope labeling and multidimensional separation for proteome and phosphoproteome quanti
Shotgun strategy based proteomics has greatly developed in recent years and nowadays it is a routine to identify and qua......
Six hybridoma cell lines that can continuously secrete monoclonal antibodies against adenylate kinase (AK) have been pro......
Huwentoxin-I, a neurotoxic peptide from the spider Selenocosmia huwena, was synthesized by sol-id-phase method with Fluo......
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Simultaneous determination of three classes of antibiotics in the suspended solids of swine wastewat
This work describes a systematic approach to the development of a method for simultaneous determination of three classes......
餐厨垃圾固相中的油脂易腐化变质,危害环境和人类健康,不利于餐厨垃圾后续资源化处理;而合理回收利用则是一种优良资源.采用微波湿......
为探究吕家坨井田地质构造格局,根据钻孔勘探资料,采用分形理论和趋势面分析方法,研究了井田7......
A solid phase radioimmunoassay for free triiodothyroninein serum was developed based on double-antibody coated tubes.The......
目的:建立同时测定鸡蛋中诺氟沙星、氧氟沙星、培氟沙星、环丙沙星、洛美沙星、达氟沙星、恩诺沙星、沙拉沙星、二氟沙星残留的固......
Simultaneous determination of three classes of antibiotics in the suspended solids of swine wastewat
This work describes a systematic approach to the development of a method for simultaneous determination of three classes......
A 1-β-methylcarbapencm analogue 6 was synthcsized on polystyrene-dicthylsilane resin (PS-DES) using 2-azetidinone beari......
传统锦州虾酱是以白虾和乌虾为原料,在高盐条件下经长时间发酵形成海产风味食品。采用HPSPME/GC-MS结合保留指数方法分析虾酱中的......
以玉米蛋白粉酶解液，控制氧化羊脂，D-木糖为主要原料，研究美拉德反应制备羊肉味风味料的最优工艺，并对羊肉味风味料的风味成分及可接受......
Peptide bond synthesis is favorable to the production of bioactive small peptides.However,the abuse of toxic reagents re......
A solid phase radioimmunoassay for free triiodothyronine in serum was developed based on double-antibody coated tubes.Th......
将纳米纤维固相萃取技术与气相色谱-火焰离子化检测器相结合,建立了同时检测油脂类食品中4种邻苯二甲酸酯（邻苯二甲酸二丁酯（ DBP）、......
本文研制了一种用于放射免疫测试的磁颗粒固相二抗分离试剂.将粗羊抗兔IgG二抗溶液纯化,采用氨基硅烷化修饰的磁性颗粒选择不同的......
目的对胸腺肽α1的固相合成工艺进行研究,并对合成产物进行活性评价.方法采用对碱敏感的Nα-芴甲氧羰基(Fmoc)作为α-氨基的保护基......
利用敌百虫在碱性介质中能够增敏鲁米诺-铁氰化钾体系产生的化学发光性能,建立了一种测定敌百虫的流动注射化学发光分析新方法,并......
为建立快速、准确的鲜食苹果中棒曲霉素含量检测方法,试验以红富士苹果为试材,分别研究不同HPLC条件对分离效果的影响,不同提取方......
建立了固相萃取前处理净化技术．高效液相色谱（HPLC）法检测枸杞中阿维菌素B1a残留量的方法。样品用乙腈提取，经C18固相萃取柱净化，采用C1......
用Amberlite XAD-2000树脂键合8-羟基喹啉固相萃取富集水中痕量铅,然后用火焰原子吸收法测定。实验了pH,样品处理速度,洗脱剂的类......
采用阴离子交换树脂为萃取剂富集、净化环境水样中氯代酚类化合物（CPS）。选取8种具有代表性的CPs，对三种不同型号、两种不同交换形式......
通过对自来水中有机污染物的检测,初步了解和评价了某市自来水中有机物污染状况.采用XAD-2树脂对水中有机物进行富集、液相色谱-质......
以NiCl2·6H1O与KBH4为原料，采用室温固相合成法，制备非晶态纳米Ni—B合金催化荆，用化学分析、XRD、TEM技术对其组成、结构和形貌......
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Laminin nonapeptide CR9 was synthesized via two different methods. A notably enhanced yield (46.8%) was obtained from me......
Resin-bound cyclic malonic ester 1 reacted with aryl isothiocynate, then was treatedwith bromine, followed by cleavage f......
A 1-β-methylcarbapencm analogue 6 was synthcsized on polystyrene-dicthylsilane resin (PS-DES) using 2-azetidinone beari......
建立一种竞争性固相放射免疫分析法（ＳＰ－ＲＩＡ），用于定量测定人体血清或脑脊髓液（ＣＳＦ）中的Ｃ－反应蛋白（Ｃ－ｒｅａｃｔｉｖｅＰｒｏｔｅｉｎ，ＣＲＰ）。最小可测量为５ｎｇ／ｍｌ；批内ＣＶ为４．９％，批间ＣＶ为１２．６％。６８份健康人血清的ＣＲＰ含量......
Solid-phase synthesis of Cu2MoS4 nanoparticles for degradation of methyl blue under a halogen-tungst
The Cu2MoS4 nanoparticles were prepared using a relatively simple and convenient solid-phase process, which was applied ......
建立了同时测定含脂羊毛中除虫脲和杀铃脲的反相高效液相色谱方法。样品用正己烷-乙醚混合溶剂提取,经凝胶渗透色谱柱和固相萃取柱......
建立了用荧光检测器同时测定11种喹诺酮类药物（包括诺氟沙星、培氟沙星、环丙沙星、恩诺沙星、氧氟沙星、达氟沙星、洛美沙星、二氟......
建立了一种基于气相色谱-离子阱二级质谱（GC-MS/MS）检测食品（薯条,薯片,咖啡,饼干和膨化食品）中丙烯酰胺残留量的方法。样品中丙烯酰胺......
采用水热法在酸处理的钛丝(Ti)基体上自制备生成了二氧化钛纳米线(TiO2NWs),接着对其在800℃进行热处理,形成了石纹状的TiO2涂层,......
Preparation of polypyrrole/nanosilica composite for solid-phase microextraction of bisphenol and pht
This paper describes the electrodeposition of polyphosphate-doped polypyrrole/nanosilica nano-composite coating on steel......
合成了作为固相微萃取（SPME）涂层的有机硅-聚氨酯共聚物，考察了该共聚物的物理性能；制备了萃取头并观察了萃取头的微观形貌，制作了SPME......
建立了环境水样中8种苯并三唑类和苯并噻唑类化合物:苯并三唑(1H-benzotriazole,BTri)、5-甲基苯并三唑(5-Methyl-1H-benzotriazol......
A method of rapidly detecting three kinds of microcystins (MCs) in environmental water samples by using disk SPE - ultra......
以赛庚啶为模板分子,甲基丙烯酸为功能单体,乙二醇二甲基丙烯酸酯为交联剂,通过优化致孔剂、单体及模板与单体摩尔比等因素,合成了......
采用固相法自组装铁基印迹聚合物（M IP）,并通过XRD与表面滴定手段对其进行表征及研究其吸附性能,结果表明：（1）M IP结晶完好,晶胞系数皆......
以萝卜为原料,以自行分离的植物乳杆菌B2进行单一菌株发酵剂接种制作萝卜泡菜产品,与完全自然发酵产品比较,通过比较发酵周期、发......
用PP-g-MMA作为增容剂对PVC/PP共混体系进行改性。用紫外光辐照接枝的方法在聚丙烯（PP）上接枝极性单体甲基丙烯酸甲酯（MMA）；讨论了光照......
Effect of Annealing Temperature and Atmosphere to Surface Solid Phase Reaction of Sapphire Substrate
The solid-phase reaction of sapphire (Al2O3) substrates and spin-coated copper nitrate films was studied. X-ray diffract......
Solid Phase Synthesis of 3,4,5-Trisubstituted-1,2,4-Triazoles Derivatives from the Resin-Bound Acylh
An extension of our methodology on solid-phase synthesis of 3,4,5-trisubstituted-1,2,4-triazoles under mild conditions h......
Multiresidue Method for Determination of 67 Pesticides in Water Samples Using Solid-Phase Extraction
A new multi-residue method based on solid-phase extraction (SPE) with centrifugation was developed for determination and......
On an example of spontaneous changes 5,7-di-tert-butylspiro (2,5) octa-4,7-diene-6-one at room temperature, a new exampl......
Integration of GC-MS Based Non-Targeted Metabolic Profiling with Headspace Solid Phase Microextracti
In this report, gas chromatography-mass spectrometry (GC-MS) based non-targeted metabolomics is used to develop appropri......
对高温固相烧结法制备锂离子电池正极材料的合成工艺进行研究．根据正交试验结果确定的最佳合成工艺条件为反应温度750℃，反应时间24h......
Microwave-assisted organic synthesis (MAOS) has attained increasing popularity due to recent advancement in the instrume......
