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The reactions of norfloxacin(H-Norf)with Mn (ClO 4 ) 2 ·6H 2 O and Mn (OH) 2 yield Mn (H-Norf)(ClO 4 ) 2 ·2H 2 O(1)and[Mn (Norf) 2 ·4H 2 O] n (2),respectively.1is monomeric while2has a novel 2D neutral square grid with an antibacterial drug as buildi ng block.Crystal data for1:triclinic,space groupP1(No.2),a=9.0939(3),b=9.4395(3),c=12.7182(3)*!,α=111.447(2),β=90.340(2),γ=112.357(1)°,V=926.34(5)*! 3 ,Z =1,ρ cacl =1.664g·cm -3 .Mo Kαradiation(λ=0.71073*!),T=293(2)K,μ=0.595mm -1 ,R 1 =0.0692,w R 2 =0.1482for 2320observed reflectio ns from 4390independent reflection s,GOF =0.940;Crystal data for2:Monoclinic,P2 1 /c,a=5.7530(12),b=21.865(4),c=13.343(3)*!,β=98.25(3)°,V=1661.1(6)*! 3 ,Z =2,ρ cacl =1.527g·cm -3 ,T=293(2)K,μ=0.477mm -1 ,R 1 =0.0531,w R 2 =0.1552for2070observed reflections from 2870independent reflections,GOF =1.384.CCDC:140819;151063.
The reactions of norfloxacin (H-Norf) with Mn (ClO 4) 2 · 6H 2 O and Mn (OH) 2 yield Mn (H-Norf) (ClO 4) 2 · 2H 2 O ) 2 · 4H 2 O] n (2), respectively.1is monomeric while2has a novel 2D neutral square grid with an antibacterial drug as buildi ng block.Crystal data for1: triclinic, space groupP1 (No.2), a = 9.0939 A = 111.447 (2), β = 90.340 (2), γ = 112.357 (1) °, V = 926.34 (5) *! 3, b = 9.4395 3, c = 12.7182 3 * , Z = 1, ρcacl = 1.664g · cm -3 .Mo Kαradiation (λ = 0.71073 *!), T = 293 (2) K, μ = 0.595 mm -1, R 1 = 0.0692, w R 2 = 0.1482 for 2320observed reflectio ns from 4390independent reflections s, GOF = 0.940; Crystal data for2: Monoclinic, P2 1 /c, a = 5.7530(12),b=21.865(4),c=13.343(3)*!,β=98.25 (3) °, V = 1661.1 (6) *! 3, Z = 2, ρcacl = 1.527g · cm -3, T = 293 (2) K, μ = 0.477mm -1, R 1 = R 2 = 0.1552 for 2070observed reflections from 2870 independent reflections, GOF = 1.384. CCDC: 1408 19; 151063.