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本文研究了在熔融的甲酸铵介质中,温度为125℃±0.5℃时应用交流示波极谱研究硝基苯等有机化合物的示波极谱特性.并且发现和采用流汞电极在1M 氢氧化钠溶液中所获得的电容切口是一样的简单.同时还发现随着电解纯化甲酸铵时间的增加.同量硝基苯产生的切口有明显地加深.提高了灵敏度.本文还使用滴汞电极、悬汞电极和 Kaliskova 电极对硝基苯进行了定性和定量.具有较高的灵敏度。重现性也较好.实验还指出.采用固体电极材料在交流示波极谱中的应用将是继续研究的新课题. ·
In this paper, we studied the oscillopolarographic properties of organic compounds such as nitrobenzene by AC oscillopolarography in a molten ammonium formate medium at a temperature of 125 ℃ ± 0.5 ℃, Sodium cuttings obtained in the capacitor incision is the same as simple.At the same time also found that with the electrolytic purification of ammonium formate time increases.The same amount of nitrobenzene incision has significantly deepened.Improved sensitivity.In this paper, Hanging mercury electrode and Kaliskova electrode nitrobenzene qualitative and quantitative. With high sensitivity. Reproducibility is better.Experiments also pointed out that the use of solid electrode materials in the AC oscilloscope polarography will continue to study a new topic.