【摘 要】
：
The title compound(S)-N-(hexahydro-2-oxo-1H-azepin-3-yl)-3-phenyl-2-propenamide(C15H18N2O2, Mr = 258.31) was synthesized by the reaction of(S)-α-amino-ε-capro
【机 构】
：
School of Pharmaceutical Sciences, Nanjing University of Technology,College of Biotechnology and Pha
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The title compound(S)-N-(hexahydro-2-oxo-1H-azepin-3-yl)-3-phenyl-2-propenamide(C15H18N2O2, Mr = 258.31) was synthesized by the reaction of(S)-α-amino-ε-caprolactam with 3-phenyl-2- propenoyl chloride. Its chemical structure was determined by 1H NMR, 13C NMR, H RMS and X-ray single-crystal diffraction. The crystal belongs to the monoclinic system, space group P21/n with a = 14.957(3), b = 4.884(1), c = 18.630(4), β = 95.91(3)o, V = 1353.7(5)3, Z = 4, Dc = 1.267 g/cm3, μ = 0.085 mm-1, F(000) = 552, R = 0.0671 and wR = 0.1547 for 2473 observed reflections with I > 2σ(I).
The title compound (S) -N- (hexahydro-2-oxo-1H-azepin-3 -yl) -3 -phenyl- 2-propenamide was synthesized by the reaction of (S) -α Its chemical structure was determined by 1H NMR, 13C NMR, H RMS and X-ray single-crystal diffraction. The crystal belongs to the monoclinic system, space group P21 / n with a = 14.957 (3) b = 4.884 (1) c = 18.630 (4) β β = 95.91 (3) o V = 1353.7 (5) 3 Z = 4 Dc = 1.267 g / cm3, μ = 0.085 mm-1, F (000) = 552, R = 0.0671 and wR = 0.1547 for 2473 observed reflections with I> 2σ (I).
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