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日本大阪Prefecture大学纳米科学与纳米技术研究中心Atsuko kosuga等人采用化学镀方法在Ca0.9Yb0.1MnO3粉末表面镀上Pd,然后进行放电等离子烧结,制出的纳米复合物表面有粒径约为50nm的Pd层,存在于Ca0.9Yb0.1MnO3基体晶界处。Pd粉中有10%(质量)磷,具有非晶态结构。含磷的镀态Pd粉经1023k烧结后转变为晶态Pd和Pd亚磷酸盐。Ca0.9
Japan Osaka Prefecture University nanoscience and nanotechnology research center Atsuko kosuga et al. Electroless plating method on Ca0.9Yb0.1MnO3 powder surface Pd, and then discharge plasma sintering, the surface of the nanocomposite particle size of about 50nm Pd layer exists at the grain boundary of Ca0.9Yb0.1MnO3 matrix. Pd powder in 10% (mass) phosphorus, with an amorphous structure. Pd-containing Pd powder is transformed into crystalline Pd and Pd phosphite after 1023k sintering. Ca0.9