【摘 要】
：
目的:建立千斤脑康宁胶囊中丹酚酸B的含量测定方法。方法:采用高效液相色谱法,kromasilC18柱(4.6 mm×250 mm,5μm),甲醇-乙腈-1%甲酸溶液(24∶10∶66)流动相,286 nm检测波长
【机 构】
：
广西中医药研究院,南宁市冠峰制药有限公司,
论文部分内容阅读
目的:建立千斤脑康宁胶囊中丹酚酸B的含量测定方法。方法:采用高效液相色谱法,kromasilC18柱(4.6 mm×250 mm,5μm),甲醇-乙腈-1%甲酸溶液(24∶10∶66)流动相,286 nm检测波长,柱温室温。结果:丹酚酸B在0.24～4.04μg,峰面积与其浓度呈良好线性关系(r=0.999 8),平均回收率97.5%,RSD 1.27%(n=6)。结论:该方法简便、准确、重复性好,可作为该制剂含量测定方法。
Objective: To establish a method for the determination of salvianolic acid B in jin jin er ning capsule. Methods: The mobile phase of kromasil C18 column (4.6 mm × 250 mm, 5 μm) and methanol-acetonitrile-1% formic acid solution (24:10:66) were used for detection of the wavelength at 286 nm. Results: There was a good linear relationship between the concentration of salvianolic acid B and its concentration (r = 0.999 8). The average recovery was 97.5% and the RSD was 1.27% (n = 6). Conclusion: The method is simple, accurate and reproducible, and can be used as a method for determination of the content of the preparation.
其他文献
以Kooijman眼模型为基础,根据Jimenez的理论及临床上应用的Munnerlyn理论,分析了激光在角膜前表面的斜入射和反射对角膜屈光手术后人眼成像质量的影响.研究表明,激光的斜入射
Background Efficient cell adhesion and proliferation is a central issue in cell-based tissue engineering, which offers great promise for repair of urethral defe
医疗激光在生物组织切割领域应用愈加广泛,但其作用效果与不良反应仍未形成统一的参数标准,对操作经验依赖严重,不便于推广;而激光参数的选择又对产品开发具有决定性意义.为
Background Ahmed glaucoma valves (AGV) has been used for decades, but there is no detailed report about the efficacy of AGV in Chinese glaucoma patients. This s
Background Quantitative magnetic resonance imaging (qMRI) of articular cartilage represents a powerful tool in osteoarthritis research, but has so far been conf
目的:比较松质骨填塞钉道、增加螺钉长度、传统聚甲基丙烯酸甲酯(polymethylmethacrylate,PMMA)强化钉道和外板开窗PMMA强化钉道四种方法翻修松动髂骨螺钉后的固定强度,探讨
为了实现网格结构零件的制造,在快速成型设备Dimetal-280上经过选区激光熔化(SLM)工艺实验,分析了SLM中能量吸收对零件尺寸的影响、激光深穿透及铺粉装置对成型效果的影响。
Background For the renal transplant recipients, anemia is one of the common complications and becomes a major medical issue before transplantation. Haemoglobin
Sondex爬行器是一种新型的测井仪器输送工具,它与常规的送进技术相比,克服了井眼弯曲使测井仪器难以下放的困难,同时也提高了测井的质量和可靠性.应用该爬行器,为套管井水平
在现代航空发动机中,广泛使用双转子加中介轴承的设计方案,以达到减轻发动机重量而提高推重比的目标.这种结构型式使发动机高、低压转子的振动特性具有很强的耦合性,而中介轴