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用磁控溅射法在Ar+N2混合气氛中制备了性能优异的具有纳米结构的Fe-Ta-N软磁薄膜。氮原子以间隙原子的形式进入纳米形态的α-Fe的晶格中,并引起了相应的晶格形变。随氮分压(pN2)的提高,α-Fe晶粒的尺寸迅速减小,在交换耦合作用下,表现出优异的软磁性能,氮分压较高时(pN27%),Ta原子和N原子将形成Ta3N5化合物相,导致薄膜软磁性能的相应降低。
Fe-Ta-N soft magnetic films with nanostructures were prepared by magnetron sputtering in Ar + N2 mixed atmosphere. The nitrogen atoms enter the lattice of α-Fe nanostructures in the form of interstitial atoms and cause the corresponding lattice deformation. With the increase of nitrogen partial pressure (pN2), the size of α-Fe grains decreases rapidly and exhibits excellent soft magnetic properties under exchange coupling. When the partial pressure of nitrogen is high (pN2 7%), Ta atoms And N atoms will form Ta3N5 compound phase, resulting in a corresponding reduction of soft magnetic properties of the film.