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The organic salt, (H2Bpy)(cda)2, was synthesized by the reaction of sodium carbamyldicyanomethanide, 4,4′-bipyridyl and manganese(Ⅱ) perchlorate in water solution. The crystal belongs to monoclinic, space group C2/c with α=20.333(7), b=6.177(2), c=15.566(