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本文提出了一个新的热化学闭路循环分解制氢的四段法.应用正交试验对影响反应收率的主要因素进行了实验.利用最小二乘方法和多元回归对实验数据进行了处理并获得了四个数学模型、利用X-射线粉末衍射对反应的中间固态物质进行了检测.研究了循环中反应的机理.
In this paper, we propose a new four-step method to decompose hydrogen in closed loop by thermochemical method. The main factors influencing the yield of the reaction were investigated by orthogonal experiments. The experimental data were processed and obtained by least square method and multiple regression Four mathematical models were used to detect the intermediate solid state of the reaction by X-ray powder diffraction, and the mechanism of the reaction was studied.