硒化合物在电子、玻璃等工业部门用途广泛，对高含量硒中碲的测定通常是用分光光度比色法或极谱法。本文详细研究了火焰原子吸收光谱法在这领域中的应用。使用本方法不必从硒化物试样中分离碲。在０．６—１．２ｍｏｌ／ＬＨＣｌ介质中测定碲时，检出限０．０８μｇ／ｍＬ，特证浓度０．１５μｇ／ｍＬ１％，线性范围１—２０μｇ／ｍＬ。相关系数０．９９９８。 Selenium compounds in the electronics, glass and other industrial sectors widely used, high content of tellurium in selenium is usually measured by spectrophotometry or polarography. In this paper, a detailed study of flame atomic absorption spectrometry in this area. There is no need to separate tellurium from the selenide sample using this method. Detection of tellurium in 0.6-1.2mol / LHCl medium, the detection limit of 0.08μg / mL, the specific concentration of 0.15μg / mL1%, linear range of 1-20μg / mL. The correlation coefficient is 0.9998.