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基于卟啉试剂TAPP与Pb ̄(2+)、Hg ̄(2+)在碱性介质中有灵敏的显色反应,建立了两次双波长分光光度法同时测定Pb、Hg的新方法,摩尔吸光系数分别为4.59×10 ̄5和4.32×10 ̄5mol ̄(-1)·cm ̄(-1)·L;可同时测定1:5~10:1范围内的Pb和Hg,用于水中Pb和Hg的同时测定,结果满意。
Based on the sensitive chromogenic reaction of TAPP with Pb ~ (2+) and Hg ~ (2+) in alkaline media, a new method of simultaneous determination of Pb and Hg by dual wavelength spectrophotometry was established. The molar absorption coefficient Respectively 4.59 × 10 -5 and 4.32 × 10 -5 mol -1 cm -1 (-1) L; simultaneous determination of Pb and Hg in the range of 1: 5 to 10: 1 can be achieved with Simultaneous determination of Pb and Hg in water with satisfactory results.