【摘 要】
：
High-quality LDH-SO4-CO3 whiskers were synthesized via liquid precipitation method using MgSO4·7H2O and Al2(SO4)3·18H2O as precursors and Na2CO3-NaHCO3 buffer solution as precipitant. The influence of buffer solution concentration on the characteristics o
【机 构】
：
School of Chemistry and Chemical Engineering, Lingnan Normal University, Zhanjiang 524048, China;Sch
【出 处】
：
武汉理工大学学报（材料科学版）（英文版）
论文部分内容阅读
High-quality LDH-SO4-CO3 whiskers were synthesized via liquid precipitation method using MgSO4·7H2O and Al2(SO4)3·18H2O as precursors and Na2CO3-NaHCO3 buffer solution as precipitant. The influence of buffer solution concentration on the characteristics of the samples was investigated. The as-grown whiskers were characterized by X-ray diffraction, transmission electron microscopy, and Brunauer-Emmett-Teller N2 specific surface area measurements. The results show that the buffer solution concentration has significant impact on whiskers with intercalated structure. The LDH-SO4-CO3 whiskers with well-defined geometry, distinct intercalated structure, decent quality, and excellent dispersing capability can be obtained under the following conditions: buffer solution volume ratio of 45％, reaction temperature of 83°C, and reaction time of 182 h. The obtained whiskers are well-crystallized and exhibit homogeneous morphology consisting of fiber bars.
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