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用引发聚合方法合成了AMPS/ AM/ AMC14S 三元共聚物。研究结果表明,在单体总浓度10 % —15 % ,AMC14S浓度0 .15 % ,pH值为中性时,在30—40℃反应8 h 可以得到转化率97% 、特性粘数10 —17 dL/g 的共聚物。通过红外光谱研究了共聚物的分子结构,并通过差热分析研究了共聚物的耐热性。
The AMPS / AM / AMC14S terpolymer was synthesized by means of initiating polymerization. The results show that the total monomer concentration of 10% -15%, AMC14S concentration of 0. 15%. When the pH value is neutral, the reaction is carried out at 30-40 ℃ for 8 h to obtain a copolymer with 97% conversion and intrinsic viscosity of 10-17 dL / g. The molecular structure of the copolymer was studied by infrared spectroscopy, and the heat resistance of the copolymer was studied by differential thermal analysis.