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目的制定全鹿丸的质量标准。方法采用薄层色谱法对方中的甘草、五味子、陈皮进行定性鉴别;采用反相高效液相色谱法测定补骨脂中补骨脂素和异补骨脂素。结果薄层色谱鉴别特征明显、专属性强;补骨脂素和异补骨脂素分别在9.75~195.00 ng、9.17~183.40 ng与峰面积有良好线性关系,平均回收率102.6%、101.5%。结论建立了全鹿丸的质量标准,定性和定量方法可靠、实用。
Purpose To establish quality standards for Quan Lu Wan. Methods TLC was used to qualitatively identify licorice, schisandra and orange peel in each other. Reversed-phase high performance liquid chromatography was used to determine psoralen and isopsoralen in psoralen. Results The identification characteristics of TLC were obvious and specific; psoralen and isopsoralen had a good linear relationship with the peak area at 9.75-195.00 ng, 9.17-183.40 ng, and the average recovery was 102.6% and 101.5%. Conclusion The quality standard of Quan Lu Wan was established, and the qualitative and quantitative methods were reliable and practical.