有机电化学合成是将电化学知识运用于有机化学中的一种合成方法。此方法克服了一般有机合成中副反应多、分离提纯困难、产物纯度不高等缺点。最重要的是一些难于用一般有机方法合成的化合物,有可能用有机电化学方法成功地合成。目前,国外有的已经把它运用于生产中,但在我国这方面报导尚未见到。就有机电化学合成方法来说,可分为恒电流电解、恒电压电解和恒电位电解。恒电位电解的优点是能保证只有唯一确定的产物。本文所述的就是运用有机电化学合成中恒电位电解法,制备高效催化剂原料(双环 Organic Electrochemical Synthesis is a synthesis method that applies electrochemical knowledge to organic chemistry. This method overcomes the general organic synthesis side reactions, separation and purification difficulties, product purity is not high and other shortcomings. The most important is that some of the compounds that are hard to synthesize by general organic methods may be successfully synthesized by using organic electrochemical methods. At present, some foreign countries have already applied it to production, but this has not been seen in our country. Organic electrochemical synthesis methods, can be divided into constant current electrolysis, constant voltage electrolysis and potentiostatic electrolysis. The advantage of potentiostatic electrolysis is that it guarantees only the only definite product. Described in this paper is the use of organic electrochemical synthesis of potentiostatic electrolysis, the preparation of efficient catalyst materials (bicyclic