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The title compound bis-9-fluorenylmethylphenyl silane (C33H26Si, Mr = 450.63) was synthesized and its structure has been synthesized and determined by X-ray analysis. The crystal is of triclinic, space group P with a = 9.478(1), b = 10.0956(1), c = 13.0243(2) ? a = 92.668(2), b = 90.809(2), g = 99.348(2)? l = 0.71073 ?, m(MoKa) = 0.115 mm-1, V = 1288.1(2) 3, Z = 2, Dc = 1.219 g/cm3 and F(000) = 476. The structure was refined to R = 0.0437 and wR(F2) = 0.0963 for 3346 observed reflections with I>2s(I). X-ray diffraction analysis reveals that the title compound is bis-9-fluorenylmethylphenyl silane.
The synthesized crystal structure of triclinic, space group P with a = 9.478 (1), b = 10.0956 (1), c = 13.0243 (2)? A = 92.668 (2), b = 90.809 (2), g = 99.348 (2)? L = 0.71073 ?, m (MoKa) = 0.115 mm-1, V = 1288.1 (2) 3, Z = 2, Dc = 1.219 g / cm3 and F (000) = 476. The structure was refined to R = 0.0437 and wR (F2) = 0.0963 for 3346 observed reflections with I> 2s X-ray diffraction analysis reveals that the title compound is bis-9-fluorenylmethylphenyl silane.