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A reverse micelle technique using non-ionic Birj 30 and n-heptane as surfactant and organic solvent,respectively,is introduced in this work to synthesize ferrous spin-crossover(SCO)nanoparticles of complex [Fe(NH2trz)3](BF4)2·H2O(FeL,NH2trz = 4-amino-1,2,4-triazole).