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A three-dimensional graphene(3DGR)was directly electrodeposited on the surface of carbon ionic liquid electrode(CILE)and further decorated by electrodeposited zinc oxide(ZnO)to get a ZnO@3DGR hybrid composite.Then myoglobin(Mb)was immobilized on the surface of composite modified electrode with a Nafion film to get the biosensor named as Nafion/Mb/ZnO@3DGR/CILE.